我是机械所的学生 做燃烧方面的 我现在需要分析燃烧後产气的particle跟tar 我找到一篇文献有提到需要用到Soxhlet apparatus 但我怕我搞错他意思 想问大家对不对 我先节录一段好了： The membrane filter with the (solid) filtration residue is extracted with 100 ml methylen chloride(CH2Cl2) in a Soxhlet apparatus at 40°C for at least 8 hours. For the extraction, preferably Soxhlet tubes made of glass fibres are used. From a defined fraction of the Soxhlet extract, the methylen chloride is carefully evaporated at approx. 40°C. The residual liquid is added to the organic phase mixture OPM. The Soxhlet residue (Solid A) is a fraction of the total particulates. 在这之前的步骤是把有机溶液（有anisole、tar跟particle）过滤 会滤出particle 我看意思好像要用索氏萃取法从filter把particle取出是吗？ 找到的原理是说易挥发溶剂在索氏提取器里不断地蒸发、冷凝、溶解被提取物、 纯溶剂再蒸发、冷凝、溶解被提取物，一直到把被提取物提取乾净 照文献看 我用的溶剂就是二氯化碳是吗？ 但我以前化学没学好 没用过这方法 不知道有人能我一些资料介绍这方法的 或是告诉我哪里能找到详尽的教学呢？ 谢谢～ -- ▁▁ ▕Eric▏ ▕Haze▏ ￣￣ --

※ 发信站: 批踢踢实业坊(ptt.cc) ◆ From: 140.112.46.189